大气与环境光学学报 ›› 2024, Vol. 19 ›› Issue (4): 456-467.doi: 10.3969/j.issn.1673-6141.2024.04.006

• 环境光学监测技术 • 上一篇    下一篇

中红外波段差分吸收检测气体池设计与实验

王怡 1, 李仕春 1,2*, 刘若彤 1, 刘家辉 1, 辛文辉 1,2   

  1. 1 西安理工大学机械与精密仪器工程学院, 陕西 西安 710048; 2 陕西省现代装备绿色制造协同创新中心, 陕西 西安 710048
  • 收稿日期:2023-01-13 修回日期:2023-03-17 出版日期:2024-07-28 发布日期:2024-07-30
  • 通讯作者: E-mail:lsczqz@xaut.edu.cn E-mail:lsczqz@xaut.edu.cn
  • 作者简介:王 怡 (2000- ), 女, 陕西西安人, 硕士研究生, 主要从事激光雷达系统集成、仪器仪表工程等方面的研究。E-mail:747156339@qq.com
  • 基金资助:
    国家自然科学基金 (62175199, 61875162), 陕西省自然科学基金 (2020JM-445), 陕西省教育厅自然科学基金 (20JY048), 陕西省大学生创 新创业训练计划项目 (S202210700104)

Design and experiment of gas cell for mid-infrared differential absorption detection

WANG Yi 1, LI Shichun 1,2*, LIU Ruotong 1, LIU Jiahui 1, XIN Wenhui 1,2   

  1. 1 School of Mechanical and Precision Instrument Engineering, Xi'an University of Technology, Xi'an 710048, China; 2 Shaanxi Collaborative Innovation Center for Modern Equipment Green Manufacturing, Xi'an 710048, China
  • Received:2023-01-13 Revised:2023-03-17 Online:2024-07-28 Published:2024-07-30

摘要: 针对中红外波段差分吸收激光雷达探测性能标定的问题, 设计并搭建了中红外波段差分吸收检测直通型气 体池, 以开展大气苯系物差分吸收光谱检测实验。以中红外带间级联激光器为光源, 结合带间级联激光器的发射光 束参数, 设计了直通型气体池的结构参数和光学参数, 测试了3187.0 nm和3235.3 nm波段的气体池透光特性和密封性 能, 并在此基础上, 以苯为例开展了差分吸收激光雷达探测标定实验。结果表明, 该气体池在测试波段的透光率大于 85%, 100 h 的负气压减少约13 kPa, 差分吸收光谱检测标定实验的相关系数为0.995, 完全满足中红外波段差分吸收 激光雷达的标定要求。

关键词: 光谱检测, 差分吸收技术, 直通型气体池, 中红外波段, 苯浓度

Abstract: To address the problem of the detection performance calibration of differential absorption lidar in mid-infrared band, a straight-through gas cell for differential absorption detection in mid-infrared band was designed and constructed to carry out experiments on differential absorption spectroscopy detection of atmospheric benzene. The structural and optical parameters of the gas cell were designed by using a midinfrared interband cascade laser as the light source and combining the emission beam parameters of the interband cascade laser. Then the transmittance characteristics and sealing performance of the gas cell were tested at 3187.0 nm and 3235.3 nm wavelengths. Finally, differential absorption lidar detection calibration experiments were carried out using benzene as an example. The results showed that the light transmission rate of the gas cell in the test band was greater than 85%, the negative air pressure was reduced by about 13 kPa after 100 h, and the correlation coefficient of the differential absorption spectroscopy detection calibration experiment was 0.995, indicating that the designed gas cell fully meets the calibration requirements of the mid infrared differential absorption lidar.

Key words: optical spectral detection, differential absorption technique, straight-through type gas cell; mid-infrared wavelength band, benzene concentration

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