大气与环境光学学报 ›› 2014, Vol. 9 ›› Issue (5): 364-369.

• 环境光学监测技术 • 上一篇    下一篇

一种X射线重金属监测仪富集样品定位方法

董欣欣, 张玉钧, 殷高方, 石朝毅, 甘婷婷, 余晓娅   

  1. (中国科学院 环境光学与技术重点实验室,中国科学院 安徽光学精密机械研究所,安徽,合肥,230031)
  • 收稿日期:2014-03-01 发布日期:2014-09-16
  • 通讯作者: 董欣欣(1990—),男(汉族),山东聊城人,硕士,主要从事光电技术方面的研究。 E-mail:xxdong@aiofm.cas.cn
  • 作者简介:董欣欣(1990—),男,汉族,山东聊城人,硕士,主要从事光电技术方面的研究。
  • 基金资助:

    国家高技术研究发展计划(863 计划)项目(2013AA065502)、安徽省科技计划项目(1206c0805012)资助

Sample Ordination Method of X-Ray Heavy Metal Monitor

DONG Xin-xin, ZHANG Yu-jun, YIN Gao-fang, SHI Chao-yi, GAN Ting-ting, YU Xiao-ya   

  1. (Key Laboratory of Environmental Optics and Technology, Anhui Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Hefei , Anhui 230031, China)
  • Received:2014-03-01 Online:2014-09-16

摘要:

X射线荧光(XRF)法是实现重金属连续监测的有效方法。为了实现工业环境大气重金属连续监测,样品的富集及与X射线测量位置的精确定位至关重要。提出了一种采用光电位移传感器检测富集样品滤纸位移,实现富集样品移动精确定位的方法。以单片机作为核心芯片,研制了该样品定位控制系统。最后,利用样品定位控制系统进行了一系列样品定位试验。实验结果显示利用光电位移传感器进行多次样品定位的相对标准偏差约为0.5%,进行100 mm位移精确定位的绝对误差小于0.8 mm,能够满足XRF大气重金属在线监测装置中的样品定位要求。

关键词: X射线荧光, 滤纸, 定位, 光电位移传感器

Abstract:

X-ray fluorescence is an effective method monitoring the heavy metals successively. To monitor the atmospheric heavy metal in factory on-line, sample enrichment and accurate control of distance between the X-ray detector and the sample are essential. An accurate distance control method, with a photoelectric displacement sensor monitoring the shift of sample, is proposed. With an MCU, the distance control system is worked out. Using the distance control system, a series of sample location control experiment are finished. The relative standard deviation of data is about 0.5%. The deviation is less than 0.8mm between the actual distance and the exact distance of 100mm. It is confirmed that this distance control system can afford the sample location requirement of the on-line monitor of the atmospheric heavy metal.

Key words: X-ray fluorescence, filter paper, location, photoelectric displacement sensor

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